<sup>31</sup>P NMR studies of diethyl phosphite derived nanocrystalline hydroxyapatite

Ben-Nissan, B; Green, DD; Kannangara, GSK; Chai, CS; Milev, A

<sup>31</sup>P NMR studies of diethyl phosphite derived nanocrystalline hydroxyapatite

Ben-Nissan, B Green, DD Kannangara, GSK Chai, CS Milev, A

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Publication Type:: Journal Article
Citation:: Journal of Sol-Gel Science and Technology, 2001, 21 (1-2), pp. 27 - 37
Issue Date:: 2001-06-01

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Field	Value	Language
dc.contributor.author	Ben-Nissan, B	en_US
dc.contributor.author	Green, DD	en_US
dc.contributor.author	Kannangara, GSK	en_US
dc.contributor.author	Chai, CS	en_US
dc.contributor.author	Milev, A	en_US
dc.date.issued	2001-06-01	en_US
dc.identifier.citation	Journal of Sol-Gel Science and Technology, 2001, 21 (1-2), pp. 27 - 37	en_US
dc.identifier.issn	0928-0707	en_US
dc.identifier.uri	http://hdl.handle.net/10453/4190
dc.description.abstract	31P nuclear magnetic resonance (NMR) spectroscopy was used to determine the structure of the intermediate species of sol derived from triethyl phosphite, calcium diethoxide and acetic acid. NMR spectral data revealed that the reaction proceeds via a dialkyl phosphite intermediate. The use of a dialkyl phosphite precursor (diethyl phosphite) with calcium diethoxide eliminated the aging time required in triethylphosphite method and offered an effective sol-gel procedure for monophasic hydroxyapatite.	en_US
dc.relation.ispartof	Journal of Sol-Gel Science and Technology	en_US
dc.relation.isbasedon	10.1023/A:1011281826850	en_US
dc.subject.classification	Materials	en_US
dc.title	<sup>31</sup>P NMR studies of diethyl phosphite derived nanocrystalline hydroxyapatite	en_US
dc.type	Journal Article
utslib.citation.volume	1-2	en_US
utslib.citation.volume	21	en_US
utslib.for	0302 Inorganic Chemistry	en_US
utslib.for	0912 Materials Engineering	en_US
pubs.embargo.period	Not known	en_US
pubs.organisational-group	/University of Technology Sydney
pubs.organisational-group	/University of Technology Sydney/Faculty of Science
pubs.organisational-group	/University of Technology Sydney/Faculty of Science/School of Chemistry and Forensic Science
pubs.organisational-group	/University of Technology Sydney/Strength - CHT - Health Technologies
utslib.copyright.status	closed_access
pubs.issue	1-2	en_US
pubs.publication-status	Published	en_US
pubs.volume	21	en_US

Abstract:

31P nuclear magnetic resonance (NMR) spectroscopy was used to determine the structure of the intermediate species of sol derived from triethyl phosphite, calcium diethoxide and acetic acid. NMR spectral data revealed that the reaction proceeds via a dialkyl phosphite intermediate. The use of a dialkyl phosphite precursor (diethyl phosphite) with calcium diethoxide eliminated the aging time required in triethylphosphite method and offered an effective sol-gel procedure for monophasic hydroxyapatite.

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http://hdl.handle.net/10453/4190