Synthesis and characterization of four alkyl 2-cyanoacrylate monomers and their precursors for use in latent fingerprint detection

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Journal Article
Journal of Polymer Science, Part A: Polymer Chemistry, 2011, 49 (1), pp. 257 - 277
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Four novel cyanoacrylates, 2-cyanoethyl 2-cyanoacrylate, 1-cyanoethyl 2-cyanoacrylate, trideuteromethyl 2-cyanoacrylate and pentadeuteroethyl 2-cyanoacrylate have been synthesized using a Diels-Alder protection/ deprotection route involving anthracene. The common route for the synthesis of alkyl 2-cyanoacrylates was found to be unsatisfactory for the production of small quantities of the targeted cyanoacrylates, which have potential as reagents for the mid-infrared spectral imaging of fingerprints on difficult surfaces. Copyright © 2010 Wiley Periodicals, Inc.
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