Determination of glyphosate and aminomethylphosphonic acid in water by LC using a new labeling reagent, 4-methoxybenzenesulfonyl fluoride

Publication Type:
Journal Article
Citation:
Chromatographia, 2010, 72 (7-8), pp. 679 - 686
Issue Date:
2010-10-01
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A rapid, low-cost, and highly sensitive analytical method to detect glyphosate and its major metabolite, aminomethylphosphonic acid (AMPA), in water samples has been developed, involving a derivatization with a new labeling reagent, 4-methoxybenzenesulfonyl fluoride, followed by reverse phase liquid chromatography with ultraviolet detection. The limits of detection of both of glyphosate and AMPA in real water samples are 0.1 μg L-1with simple pre-concentration. This method has proven to be sensitive and reliable for determination of glyphosate and AMPA in water samples. © 2010 Vieweg+Teubner Verlag | Springer Fachmedien Wiesbaden GmbH.
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