From Lead(II) Dithiocarbamate Precursors to a Fast Response PbS Positive Temperature Coefficient Thermistor

Angeloski, A; Gentle, AR; Scott, JA; Cortie, MB; Hook, JM; Westerhausen, MT; Bhadbhade, M; Baker, AT; McDonagh, AM

From Lead(II) Dithiocarbamate Precursors to a Fast Response PbS Positive Temperature Coefficient Thermistor

Angeloski, A

Gentle, AR

Scott, JA Cortie, MB

Hook, JM Westerhausen, MT Bhadbhade, M Baker, AT

McDonagh, AM

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Publication Type:: Journal Article
Citation:: Inorganic Chemistry, 2018, 57 (4), pp. 2132 - 2140
Issue Date:: 2018-02-19

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Field	Value	Language
dc.contributor.author	Angeloski, A https://orcid.org/0000-0003-4395-1829	en_US
dc.contributor.author	Gentle, AR https://orcid.org/0000-0001-8964-0722	en_US
dc.contributor.author	Scott, JA	en_US
dc.contributor.author	Cortie, MB https://orcid.org/0000-0003-3202-6398	en_US
dc.contributor.author	Hook, JM	en_US
dc.contributor.author	Westerhausen, MT	en_US
dc.contributor.author	Bhadbhade, M	en_US
dc.contributor.author	Baker, AT https://orcid.org/0000-0001-9700-0178	en_US
dc.contributor.author	McDonagh, AM https://orcid.org/0000-0002-9502-1175	en_US
dc.date.issued	2018-02-19	en_US
dc.identifier.citation	Inorganic Chemistry, 2018, 57 (4), pp. 2132 - 2140	en_US
dc.identifier.issn	0020-1669	en_US
dc.identifier.uri	http://hdl.handle.net/10453/132944
dc.description.abstract	© 2018 American Chemical Society. PbS submicron crystals were formed by thermolysis of two different lead dithiocarbamate complexes. These precursors were readily synthesized and fully characterized, and in situ synchrotron powder diffraction experiments were performed to characterize their decomposition. The structure and purity of resultant PbS was examined using scanning electron and transmission electron microscopies, powder X-ray diffraction, and infrared spectroscopy. Submicron crystalline PbS was used to create a new PbS thermistor with excellent sensitivity and an ultrarapid thermal response time.	en_US
dc.relation.ispartof	Inorganic Chemistry	en_US
dc.relation.isbasedon	10.1021/acs.inorgchem.7b03009	en_US
dc.subject.classification	Inorganic & Nuclear Chemistry	en_US
dc.title	From Lead(II) Dithiocarbamate Precursors to a Fast Response PbS Positive Temperature Coefficient Thermistor	en_US
dc.type	Journal Article
utslib.citation.volume	4	en_US
utslib.citation.volume	57	en_US
utslib.for	0302 Inorganic Chemistry	en_US
utslib.for	0399 Other Chemical Sciences	en_US
utslib.for	0306 Physical Chemistry (incl. Structural)	en_US
pubs.embargo.period	Not known	en_US
pubs.organisational-group	/University of Technology Sydney
pubs.organisational-group	/University of Technology Sydney/Faculty of Science
pubs.organisational-group	/University of Technology Sydney/Faculty of Science/School of Mathematical and Physical Sciences
pubs.organisational-group	/University of Technology Sydney/Strength - CCET - Centre for Clean Energy Technology
pubs.organisational-group	/University of Technology Sydney/Students
utslib.copyright.status	closed_access
pubs.issue	4	en_US
pubs.publication-status	Published	en_US
pubs.volume	57	en_US

Abstract:

© 2018 American Chemical Society. PbS submicron crystals were formed by thermolysis of two different lead dithiocarbamate complexes. These precursors were readily synthesized and fully characterized, and in situ synchrotron powder diffraction experiments were performed to characterize their decomposition. The structure and purity of resultant PbS was examined using scanning electron and transmission electron microscopies, powder X-ray diffraction, and infrared spectroscopy. Submicron crystalline PbS was used to create a new PbS thermistor with excellent sensitivity and an ultrarapid thermal response time.

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http://hdl.handle.net/10453/132944