Synthesis of functional oxides by a novel mechanical milling-electric discharge method

Needham, SA; Calka, A; Wang, G; Peleckis, G; Liu, H

Synthesis of functional oxides by a novel mechanical milling-electric discharge method

Needham, SA Calka, A Wang, G

Peleckis, G Liu, H

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Publication Type:: Journal Article
Citation:: Journal of Materials Chemistry, 2006, 16 (46), pp. 4488 - 4493
Issue Date:: 2006-01-01

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Field	Value	Language
dc.contributor.author	Needham, SA	en_US
dc.contributor.author	Calka, A	en_US
dc.contributor.author	Wang, G https://orcid.org/0000-0003-4295-8578	en_US
dc.contributor.author	Peleckis, G	en_US
dc.contributor.author	Liu, H	en_US
dc.date.issued	2006-01-01	en_US
dc.identifier.citation	Journal of Materials Chemistry, 2006, 16 (46), pp. 4488 - 4493	en_US
dc.identifier.issn	0959-9428	en_US
dc.identifier.uri	http://hdl.handle.net/10453/14648
dc.description.abstract	Functional metal oxide powders (LiCoO<inf>2</inf>, LiFePO<inf>4</inf>, SrTi<inf>1-x</inf>Co<inf>x</inf>O<inf>3</inf>) have been synthesized by a novel Electric Discharge Assisted Mechanical Milling (EDAMM) processing technique. Characterisation of the as-synthesized powders by XRD, SEM, and TEM confirm near pure phases with a highly controllable morphology can be produced in only minutes. The electrochemical (LiCoO<inf>2</inf>, LiFePO<inf>4</inf>) and magnetic (SrTi<inf>1-x</inf>Co<inf>x</inf>O<inf>3</inf>) behaviour of the powders indicates functionality that at least matches that of powders synthesized by traditional solid-state approaches. The EDAMM technique provides significant commercial opportunities as the method has proven to be scalable and powder morphologies can be made to order. © The Royal Society of Chemistry.	en_US
dc.relation.ispartof	Journal of Materials Chemistry	en_US
dc.relation.isbasedon	10.1039/b608437k	en_US
dc.subject.classification	Nanoscience & Nanotechnology	en_US
dc.title	Synthesis of functional oxides by a novel mechanical milling-electric discharge method	en_US
dc.type	Journal Article
utslib.citation.volume	46	en_US
utslib.citation.volume	16	en_US
utslib.for	0912 Materials Engineering	en_US
utslib.for	03 Chemical Sciences	en_US
utslib.for	09 Engineering	en_US
pubs.embargo.period	Not known	en_US
pubs.organisational-group	/University of Technology Sydney
pubs.organisational-group	/University of Technology Sydney/Faculty of Science
pubs.organisational-group	/University of Technology Sydney/Faculty of Science/School of Mathematical and Physical Sciences
pubs.organisational-group	/University of Technology Sydney/Strength - CCET - Centre for Clean Energy Technology
utslib.copyright.status	closed_access
pubs.issue	46	en_US
pubs.publication-status	Published	en_US
pubs.volume	16	en_US

Abstract:

Functional metal oxide powders (LiCoO2, LiFePO4, SrTi1-xCoxO3) have been synthesized by a novel Electric Discharge Assisted Mechanical Milling (EDAMM) processing technique. Characterisation of the as-synthesized powders by XRD, SEM, and TEM confirm near pure phases with a highly controllable morphology can be produced in only minutes. The electrochemical (LiCoO2, LiFePO4) and magnetic (SrTi1-xCoxO3) behaviour of the powders indicates functionality that at least matches that of powders synthesized by traditional solid-state approaches. The EDAMM technique provides significant commercial opportunities as the method has proven to be scalable and powder morphologies can be made to order. © The Royal Society of Chemistry.

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http://hdl.handle.net/10453/14648