The performance of second generation silica monoliths, operating in parallel segmented flow mode

Soliven, A; Foley, D; Pereira, L; Pravadali-Cekic, S; Dennis, GR; Cabrera, K; Ritchie, H; Edge, T; Shalliker, RA

The performance of second generation silica monoliths, operating in parallel segmented flow mode

Soliven, A Foley, D Pereira, L Pravadali-Cekic, S Dennis, GR Cabrera, K Ritchie, H Edge, T Shalliker, RA

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Publisher:: Elsevier BV
Publication Type:: Journal Article
Citation:: Microchemical Journal, 2016, 124, pp. 657-661
Issue Date:: 2016-01-01

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Field	Value	Language
dc.contributor.author	Soliven, A
dc.contributor.author	Foley, D
dc.contributor.author	Pereira, L
dc.contributor.author	Pravadali-Cekic, S
dc.contributor.author	Dennis, GR
dc.contributor.author	Cabrera, K
dc.contributor.author	Ritchie, H
dc.contributor.author	Edge, T
dc.contributor.author	Shalliker, RA
dc.date.accessioned	2022-08-14T02:19:20Z
dc.date.available	2022-08-14T02:19:20Z
dc.date.issued	2016-01-01
dc.identifier.citation	Microchemical Journal, 2016, 124, pp. 657-661
dc.identifier.issn	0026-265X
dc.identifier.uri	http://hdl.handle.net/10453/160114
dc.description.abstract	This study investigates the chromatographic performance of second generation monoliths in its conventional design, as well as replacing the standard outlet with an Active Flow Technology (AFT) assembly to minimise inefficient flow contributions. The AFT coupled monolith resulted in up to 50% improvement on the conventional monolith's efficiency and a 16% improvement in sensitivity. Exploitation of the current second generation monolith's silica infrastructure and AFT coupling in the parallel segmented flow (PSF) mode of operation would benefit high through-put analyses that demand highly efficient, sensitive, low volume detection, front end separation solutions utilizing conventional HPLC systems.
dc.language	en
dc.publisher	Elsevier BV
dc.relation.ispartof	Microchemical Journal
dc.relation.isbasedon	10.1016/j.microc.2015.08.022
dc.rights	info:eu-repo/semantics/closedAccess
dc.subject	0301 Analytical Chemistry
dc.subject.classification	Analytical Chemistry
dc.title	The performance of second generation silica monoliths, operating in parallel segmented flow mode
dc.type	Journal Article
utslib.citation.volume	124
utslib.for	0301 Analytical Chemistry
pubs.organisational-group	/University of Technology Sydney
pubs.organisational-group	/University of Technology Sydney/Faculty of Science
pubs.organisational-group	/University of Technology Sydney/Faculty of Science/School of Mathematical and Physical Sciences
utslib.copyright.status	closed_access	*
dc.date.updated	2022-08-14T02:19:19Z
pubs.publication-status	Published
pubs.volume	124

Abstract:

This study investigates the chromatographic performance of second generation monoliths in its conventional design, as well as replacing the standard outlet with an Active Flow Technology (AFT) assembly to minimise inefficient flow contributions. The AFT coupled monolith resulted in up to 50% improvement on the conventional monolith's efficiency and a 16% improvement in sensitivity. Exploitation of the current second generation monolith's silica infrastructure and AFT coupling in the parallel segmented flow (PSF) mode of operation would benefit high through-put analyses that demand highly efficient, sensitive, low volume detection, front end separation solutions utilizing conventional HPLC systems.

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http://hdl.handle.net/10453/160114