Characterization of nanometer-sized VO2 nanoparticles prepared by an aqueous route

Publisher:
Australian Institute of Physics
Publication Type:
Conference Proceeding
Citation:
Proceedings of the 31st Annual Condensed Matter and Materials Meeting, 2007, pp. 1 - 3
Issue Date:
2007-01
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We describe a convenient aqueous route to prepare VO2, based on the reductive precipitation of vanadium dioxide VO2 from a vanadate solution. The effect of the reaction conditions is systematically studied, and a protocol to optimize the production of VO2 while minimizing the appearance of other compounds is presented. The products were characterized using calorimetry, X-ray diffraction and high-resolution scanning electron microscopy.
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